STANNOUS IODIDE HCL IN TETRAHYDROFURAN - A NEW SYSTEM FOR THE REDUCTION OF VARIOUS NITRO-COMPOUNDS - MILD CONVERSION OF 6-NITRO-DELTA(5)-STEROIDS TO 6-KETO-STEROIDS
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STANNOUS IODIDE HCL IN TETRAHYDROFURAN - A NEW SYSTEM FOR THE REDUCTION OF VARIOUS NITRO-COMPOUNDS - MILD CONVERSION OF 6-NITRO-DELTA(5)-STEROIDS TO 6-KETO-STEROIDS
Bordoloi, M.; Singhal, G.M.; Das, N.B.; Sharma, R.P.
It has been shown that 6-nitro-DELTA5-steroids, nitrostyrene and saturated aliphatic nitro compounds in tetrahydrofuran are reduced efficiently with stannous iodide and a catalytic amount of concentrated hydrochloric acid to the corresponding 6-ketosteroids, oximes or hydroxylamine derivatives in good yields, respectively.
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