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Studies on ferric oxide hydroxides .2. Structural properties of goethite samples (alpha-FeOOH) prepared by homogeneous precipitation from Fe(NO3)(3) solution in the presence of sulfate ions

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dc.contributor.author Parida, K.
dc.contributor.author Das, J.
dc.date.accessioned 2018-10-01T12:19:59Z
dc.date.available 2018-10-01T12:19:59Z
dc.date.issued 1996
dc.identifier.citation Journal Of Colloid And Interface Science, 178(2), 1996: 586-593
dc.identifier.issn 0021-9797
dc.identifier.uri http://ore.immt.res.in/handle/2018/542
dc.description.abstract A series of goethite samples (alpha-FeOOH) have been prepared by homogeneous precipitation from Fe(NO3)(3) solution in the presence of SO4-2 ions and characterized by various techniques. Although the cell parameters, cell volumes, and crystallite sizes of all the samples prepared under different conditions remain almost same, the surface area, micropore-mesopore ratio, pore volume, pore radius, particle size, and surface acidity are influenced by SO4-2/Fe+3 ratio, initial pH, and temperature of hydrolysis. The sample prepared at SO4-2/Fe+3 ratio of 0.5, initial pH of 1.5, and hydrolysis temperature of 90 degrees C has predominantly micropores and possesses high surface area (133.5 m(2)/g) and acid sites (100 mu mol/g). (C) 1996 Academic Press, Inc.
dc.language en
dc.publisher Academic Press
dc.relation.isreferencedby SCI
dc.rights Copyright [1996]. All efforts have been made to respect the copyright to the best of our knowledge. Inadvertent omissions, if brought to our notice, stand for correction and withdrawal of document from this repository.
dc.subject Chemical Sciences
dc.title Studies on ferric oxide hydroxides .2. Structural properties of goethite samples (alpha-FeOOH) prepared by homogeneous precipitation from Fe(NO3)(3) solution in the presence of sulfate ions
dc.type Journal Article
dc.affiliation.author CSIR-IMMT, Bhubaneswar 751013, Odisha, India


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