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Surfactant directed synthesis of mesoporous alumina and alpha-alumina single crystal

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dc.contributor.author Mishra, G.
dc.contributor.author Dash, B.
dc.contributor.author Dash, A.
dc.contributor.author Bhattacharya, I.N.
dc.date.accessioned 2018-10-01T12:26:38Z
dc.date.available 2018-10-01T12:26:38Z
dc.date.issued 2016
dc.identifier.citation Crystal Research And Technology, 51(7), 2016: 433-440
dc.identifier.issn 0232-1300
dc.identifier.uri http://ore.immt.res.in/handle/2018/2298
dc.description.abstract Mesoporous Al2O3 were positively synthesized via treatment of the freshly precipitated amorphous alumina gel using aluminium sulphate as aluminium source, and sodium dodecyl sulphate (SDS) as structure-directing agent (SDAs). The microstructures, morphologies and textural properties of the as-prepared materials were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM) and thermo gravimetric analysis (TG-DTA). The calcined product at 600 degrees C was highly porous in nature having a BET surface area of 42m(2)/g. These porous Al2O3 exhibits excellent adsorption performance for Congo red and the corresponding decolourisation efficiencies reached 99% in just 15 min at 27 degrees C. The subsequent calcined product at 1200 degrees C is the alpha alumina single crystal hexagonal platelets with rhombohedral crystallization.
dc.language en
dc.publisher Wiley
dc.relation.isreferencedby SCI
dc.rights Copyright [2016]. All efforts have been made to respect the copyright to the best of our knowledge. Inadvertent omissions, if brought to our notice, stand for correction and withdrawal of document from this repository.
dc.subject Chemical Sciences
dc.title Surfactant directed synthesis of mesoporous alumina and alpha-alumina single crystal
dc.type Journal Article
dc.affiliation.author CSIR-IMMT, Bhubaneswar 751013, Odisha, India


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