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Amine functionalized layered double hydroxide: a reusable catalyst for aldol condensation

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dc.contributor.author Sahoo, M.
dc.contributor.author Singha, S.
dc.contributor.author Parida, K.M.
dc.date.accessioned 2018-10-01T12:24:49Z
dc.date.available 2018-10-01T12:24:49Z
dc.date.issued 2011
dc.identifier.citation New Journal Of Chemistry, 35(11), 2011: 2503-2509
dc.identifier.issn 1144-0546
dc.identifier.uri http://ore.immt.res.in/handle/2018/1629
dc.description.abstract Zn : Al layered double hydroxide-supported 3-aminopropyltriethoxysilane (APTES) and N-methyl 3-aminopropyltriethoxy silane (MAPTES) are found to be efficient, environmentally attractive and selective solid base catalysts for liquid phase aldol condensation reactions at room temperature. The organic functionalized solid catalysts were characterized by XRD, FT-IR, Raman, EDX, SEM, TG -DTA, (13)C and (29)Si CP MAS NMR techniques. The XRD pattern indicated the anti-parallel monolayer arrangements of organic moieties in the interlayer space of LDH. (29)Si NMR confirmed that the linking silicon atom is fully condensed in the framework. The reusability study shows consistent activity of the heterogeneous catalyst after several cycles.
dc.language en
dc.publisher Royal Society Of Chemistry
dc.relation.isreferencedby SCI
dc.rights Copyright [2011]. All efforts have been made to respect the copyright to the best of our knowledge. Inadvertent omissions, if brought to our notice, stand for correction and withdrawal of document from this repository.
dc.subject Chemical Sciences
dc.title Amine functionalized layered double hydroxide: a reusable catalyst for aldol condensation
dc.type Journal Article
dc.affiliation.author CSIR-IMMT, Bhubaneswar 751013, Odisha, India


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