| dc.contributor.author |
Parida, K.M. |
|
| dc.contributor.author |
Mallick, S. |
|
| dc.contributor.author |
Sahoo, P.C. |
|
| dc.contributor.author |
Rana, S.K. |
|
| dc.date.accessioned |
2018-10-01T12:23:29Z |
|
| dc.date.available |
2018-10-01T12:23:29Z |
|
| dc.date.issued |
2010 |
|
| dc.identifier.citation |
Applied Catalysis A-General, 381(1-2), 2010: 226-232 |
|
| dc.identifier.issn |
0926-860X |
|
| dc.identifier.uri |
http://ore.immt.res.in/handle/2018/1505 |
|
| dc.description |
CSIR |
|
| dc.description.abstract |
Amine-functionalized mesoporous zirconia was prepared by a co-condensation method using silane (aminopropyltrimethoxysilane, APTES) and zirconium butoxide. The materials were characterized by Xray diffraction, BET surface area analysis, (13)C magic angle spinning-nuclear magnetic resonance (NMR), Fourier-transfer infrared spectroscopy (FTIR), transmittance electron micrography (TEM), and CHN analysis. FTIR and NMR results revealed the successful grafting of organic amines onto the surface of zirconia. The catalytic activities were investigated for liquid phase Knoevenagel condensation of various aromatic aldehydes with diethyl malonate. The catalysts showed excellent yield of products at room temperature in solvent-free condition. (C) 2010 Elsevier B.V. All rights reserved. |
|
| dc.language |
en |
|
| dc.publisher |
Elsevier |
|
| dc.relation.isreferencedby |
SCI |
|
| dc.rights |
Copyright [2010]. All efforts have been made to respect the copyright to the best of our knowledge. Inadvertent omissions, if brought to our notice, stand for correction and withdrawal of document from this repository. |
|
| dc.subject |
Chemical Sciences |
|
| dc.subject |
Interdisciplinary Sciences |
|
| dc.title |
A facile method for synthesis of amine-functionalized mesoporous zirconia and its catalytic evaluation in Knoevenagel condensation |
|
| dc.type |
Journal Article |
|
| dc.affiliation.author |
CSIR-IMMT, Bhubaneswar 751013, Odisha, India |
|