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Cesium salts of heteropoly acid immobilized mesoporous silica: An efficient catalyst for acylation of anisole

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dc.contributor.author Parida, K.M.
dc.contributor.author Rana, S.
dc.contributor.author Mallick, S.
dc.contributor.author Rath, D.
dc.date.accessioned 2018-10-01T12:23:22Z
dc.date.available 2018-10-01T12:23:22Z
dc.date.issued 2010
dc.identifier.citation Journal Of Colloid And Interface Science, 350(1), 2010: 132-139
dc.identifier.issn 0021-9797
dc.identifier.uri http://ore.immt.res.in/handle/2018/1478
dc.description CSIR
dc.description.abstract A series of Cs salt of phosphotungstic acid (Cs-PTA) supported on MCM-41 (Cs-PTA/MCM-41) was synthesized by a wet impregnation method and thoroughly characterized by using various analytical techniques, viz. X-ray diffraction, UV-Vis diffused reflectance spectroscopy (UV-Vis DRS), nitrogen adsorption desorption, scanning electron microscopy (SEM), Infrared spectra (FTIR), temperature programmed reduction (TPR), and temperature programmed desorption (TPD). The spectroscopic results revealed that Cs-PTA is highly dispersed on a MCM-41 surface. The 50 wt.% Cs-PTA supported on MCM-41 showed remarkable catalytic performance toward acylation of anisole reaction. The catalyst is regenerable by simple calcinations without appreciable loss in catalytic activity. (C) 2010 Elsevier Inc. All rights reserved.
dc.language en
dc.publisher Elsevier
dc.relation.isreferencedby SCI
dc.rights Copyright [2010]. All efforts have been made to respect the copyright to the best of our knowledge. Inadvertent omissions, if brought to our notice, stand for correction and withdrawal of document from this repository.
dc.subject Chemical Sciences
dc.title Cesium salts of heteropoly acid immobilized mesoporous silica: An efficient catalyst for acylation of anisole
dc.type Journal Article
dc.affiliation.author CSIR-IMMT, Bhubaneswar 751013, Odisha, India


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