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Synthesis of high-surface area Mn-doped barium hexa-aluminates by a combination of hydrothermal precipitation-calcination route

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dc.contributor.author Mishra, D.
dc.contributor.author Anand, S.
dc.contributor.author Panda, R.K.
dc.contributor.author Das, R.P.
dc.date.accessioned 2018-10-01T12:22:02Z
dc.date.available 2018-10-01T12:22:02Z
dc.date.issued 2003
dc.identifier.citation Materials Chemistry And Physics, 82(3), 2003: 892-896
dc.identifier.issn 0254-0584
dc.identifier.uri http://ore.immt.res.in/handle/2018/1045
dc.description.abstract High-surface area (25 m(2) g(-1)) Mn-doped barium hexa-aluminates with compositions BaMnAl11O19 and BaMn2Al10O19 were prepared by a combination of hydrothermal precipitation-calcination route. The precursors of the above two compounds were obtained by hydrolyzing a mixture of aqueous solutions of Ba, Al, and Mn at 180 degreesC for 1 h in the presence of urea. The analysis of the hydrothermally prepared samples showed the presence of carbonate and/or hydroxide phases of Ba and Mn and boebmite. Barium mono-aluminate (BaAl2O4), Ba-beta(II)-Al2O3, gamma-Al2O3, and a small fraction of MnO2 were observed after calcination of these hydrothermally prepared precursors at 1200degreesC. A mixture of Ba-beta(1)-Al2O3 and Ba-beta(II)-Al2O3 phases were found after calcination at 1400degreesC for 2 h with no other oxide phases of Ba, Al or Mn. (C) 2003 Elsevier B.V. All rights reserved.
dc.language en
dc.publisher Elsevier
dc.relation.isreferencedby SCI
dc.rights Copyright [2003]. All efforts have been made to respect the copyright to the best of our knowledge. Inadvertent omissions, if brought to our notice, stand for correction and withdrawal of document from this repository.
dc.subject Materials Sciences
dc.title Synthesis of high-surface area Mn-doped barium hexa-aluminates by a combination of hydrothermal precipitation-calcination route
dc.type Journal Article
dc.affiliation.author CSIR-IMMT, Bhubaneswar 751013, Odisha, India


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